Quality assurance of soft drinks and juices by color measurements

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1 Quality assurance of soft drinks and juices by color measurements Dieses Dokument ist Eigentum des KRONES Konzerns und enthält interne Informationen. Es darf nur zu den vereinbarten Zwecken verwendet werden. Die Vervielfältigung und Weitergabe an Dritte ist nicht gestattet. Datum: Empfänger: Erstellt von: Dr. Roland Feilner

2 2 krones: Beispieltext Theoretical basics thermal fruit juice processing Preservation of juices through thermal treatment deactivation of enzymes and destroying of microorganism Temperature and time: so much as necessary and so less as possible sec. at C The thermal impact helps to achieve a high durability -> also the thermal impact destroys important ingredients (Vitamin etc.) -> and change the visual and testable matrix of the juice

3 3 krones: Beispieltext Color and color change Color in orange juice through carotenoid safe through Vitamin C (oxidation) Color change in the juice during the thermal impact through maillard reactions building of brown Melanoidine β-carotin

4 4 krones: Beispieltext Orange juice Sample drawing during the runnig production at three different process steps -> increasing thermal impact of the samples 1. Tank before heating (VE) 2. Tank after heating (NE) 3. Hot Bottled juice 0,7 l- (FL)

5 5 krones: Beispieltext Measurement equipment ColorLite sph 850 Wavelength range nm Radiation of the samples with defined LED-Light Measurement of the remitted light Edit of the three color values L*a*b* calculation of ΔE color distance to the untreated sample )

6 6 krones: Beispieltext visual expertise orange juice At 20 min optical diffence visible

7 7 krones: Beispieltext Analysis The sample treatment groups into two phases first the up heating from 20 to 95 C in 20 sec. and second the heat holding phase by 95 C and 30 minutes

8 8 krones: Beispieltext Wavelength range 545 nm Clear classification sample VE / NE & FL No significant different between the samples NE and FL

9 9 krones: Beispieltext L*- value sample VE shows a higher level than sample NE and FL No interpretable results between the samples NE and FL Only sample VE shows a significant darker color over the thermal impact

10 10 krones: Beispieltext a*-value Clear color different measurable by a- value detection No significant different between the samples measurably (no influence of the thermal impact before)

11 11 krones: Beispieltext b*-value All samples shows first an increasing than an decreasing Also the start level is not to interpret

12 12 krones: Beispieltext ΔE-value ) Biggest different by sample VE (without thermal impact) Graphs are at close quarters color change independent from the thermal impact No clearly interpretation possible

13 13 krones: Beispieltext Summary Analysis Clear color different measurable by a- value detection Measurable of the thermal impact only by the sample VE and NE (L-value and 545nm) Not measurable of the thermal impact by the sample FL (no more different) B-value and deltae shows no usable results For the practical time levels (30 90 sec.) of the thermal treatment plants with a following cooler the measurement shows no usable answers.

14 14 krones: Beispieltext literature Birus, T. (2001). Moderne Apfelsaft-Technologie - Das Fruchtsaft-Fachbuch für den Praktiker. Schönborn: Flüssiges Obst GmbH Ringblom, U. (2004). The Orange Book. Lund, Sweden: Tetra Pak Processing Systems AB Schobinger, U. (2001). Frucht- und Gemüsesäfte. Stuttgart: Eugen Ulmer GmbH & Co. Ashrust, P. (1999). Production And Packiaging Of Non-Carbonated Fruit Juices And Fruit Beverages". New York: Aspen Publishers, Inc Bild Messzelle: Perkin Elmer Lambda 35: Manual Labsphere RSA-PE-20 Seite 7 Bild Phloretin: Cvf-ps. (11. November 2007). Wikipedia. Abgerufen am 20. Oktober 2013 von de.m.wikipedia.org/wiki/datei:phloretin.png Bild Catechin: Neurotiker. (8. August 2008). Wikipedia. Abgerufen am 25.. Oktober 2013 von de.m.wikipedia.org/wiki/datei:(-)-catcechin.svg Bild β-carotin: Neurotiker. (1.Juli 2007). Wikipedia. Abgerufen am von commons.wikimedia.org/wiki/file:beta-carotin.svg Bild Pasteurisationsbedingungen für einige Fruchtsäfte : Schobinger, U. (2001). Frucht- und Gemüsesäfte. Stuttgart: Eugen Ulmer GmbH & Co; Seite 300

15 [2] Thanks to you for your attention and Kilian Viertel & the Beuth Hochschule Berlin for the interesting results!

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