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Horst Burgstaller
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1 ANALYSIS REPORT No DATE: PAGE 1/ ANALYSIS REQUESTED: Tetracyclines by LC-MS/MS ( ) Oxytetracycline n.d. µg/kg PM DE01_060/116 (a) 1 Tetracycline n.d. µg/kg PM DE01_060/116 (a) 1 Chlortetracycline n.d. µg/kg PM DE01_060/116 (a) 1 Doxycycline n.d. µg/kg PM DE01_060/116 (a) 1 Demeclocycline n.d. µg/kg PM DE01_060/116 (a) 1 Methacycline n.d. µg/kg PM DE01_060/116 (a) 1 Minocycline n.d. µg/kg PM DE01_060/116 (a) 1 n.d. - not detected < limit of quantification 10 µg/kg Regarding the examined parameters and the mentioned limit of quantification the sample corresponds to the legal regulations (regulation (EC) 470/2009 in conjunction with regulation (EU) 37/2010 (dated Feb. 9th 2010)). The results are stated as sum of the parent drug and the corresponding 4-Epimer. Martin Linkogel Head of Laboratory, Certified Food Chemist

2 ANALYSIS REPORT No DATE: PAGE 1/ ANALYSIS REQUESTED: Streptomycin by LC-MS/MS ( ) Streptomycin n.d. µg/kg PM DE01_104 (a) 1 Dihydrostreptomycin n.d. µg/kg PM DE01_104 (a) 1 n.d. - not detected < 10 µg/kg limit of quantification Regarding the examined parameters and the mentioned limit of quantification the sample corresponds to the legal regulations (regulation (EC) 470/2009 in conjunction with regulation (EU) 37/2010 (dated Feb. 9th 2010)). Martin Linkogel Head of Laboratory, Certified Food Chemist

3 ANALYSIS REPORT No DATE: PAGE 1/ ANALYSIS REQUESTED: Commercial Analysis ( ) HMF 10.8 mg/kg PM DE01_021 (a) 1 Moisture content 17.7 % PM DE01_029 (a) 2 ph 3.8 ph PM DE01_042 (a) 3 Diastase 26.4 DZ PM DE01_090 (a) 4 Free acid 33.2 mmol/kg PM DE01_042 (a) 3 HMF: n.d.- not detectable < limit of quantification 0.1 mg/kg Diastase: n.d. - not detected < limit of quantification 0.1 DZ Free Acid: n.b. - not detectable < limit of quantification 0,1 mmol/kg (a) : accredited under terms of DIN EN ISO/IEC (na) : not accredited method. (1) DIN mod. (2) ASU 64 LFGB L mod. (3) Inhouse procedure (4) Inhouse procedure Regarding the examined parameters the sample corresponds to the legal regulations (Honey directive 2001/110/EC from Dec. 20th, 2001; Article 1 in connection with Annex II). Dr. Christof Kunert Responsible Scientist

4 ANALYSIS REPORT No DATE: PAGE 1/ Packaging / Quantity : Plastic container, twist off / ca.130g Start / End of analysis : / ANALYSIS REQUESTED: 13C Isotope Analysis (EA-IRMS) C4 Sugar in Honey ( ) Protein (P) d13c(%o) PM DE01_026 (a) 1 Honey (H) d13c(%o) PM DE01_026 (a) 1 Difference (P - H) 1.6 d13c(%o) PM DE01_026 (a) 1 C4-sugar 0.0 % PM DE01_026 (a) 1 n.a.: not analyzed; n.d.: not detected; d13c value in permil. vs. V-PDB standard SPECIFICATIONS C4 < 7 %: the sample is not adulterated with C4 sugars; C4 >= 7 %: the sample is adulterated with C4 sugars (a) : accredited under terms of DIN EN ISO/IEC (na) : not accredited method. (1) AOAC The result does not indicate an addition of sugar issued from C4 plants (according to AOAC method ; Journal of AOAC International 1995, revision March 1999, chapter 44, p ). Regarding the examined parameter the sample corresponds to the legal regulations. (2001/110/EC dated Dec. 20th, 2001; Article 1connected with Annex II). Dr. Silke Schimanski Responsible Scientist, Certified Food Chemist

5 ANALYSIS REPORT No DATE: PAGE 1/ Packaging / Quantity : Plastic container, twist off / ca.130g Start / End of analysis : / ANALYSIS REQUESTED: Sugar spectrum by HPLC-RI ( ) Fructose (F) 39.3 g/100 g PM DE01_020 (a) 1 Glucose (G) 31.8 g/100 g PM DE01_020 (a) 1 Sucrose n.d. g/100 g PM DE01_020 (a) 1 Turanose n.d. g/100 g PM DE01_020 (a) 1 Maltose 1.1 g/100 g PM DE01_020 (a) 1 F/G ratio* 1.24 PM DE01_020 (a) 1 Invert sugar (F+G)* 71.1 g/100 g PM DE01_020 (a) 1 n.d. - not detected < 0.5 g/100 g (Fru, Glu, Suc); < 1.0 g/100 g (Mal, Tur); *calculated (a) : accredited under terms of DIN EN ISO/IEC (na) : not accredited method. (1) ASU 64 LFGB L Regarding the analyzed parameters and the mentioned limits of detection the sugar content of the sample corresponds to the legal regulations (Honey directive 2001/110/EC from Dec. 20th, 2001; Article 1 in connection with Annex II). The F/G ratio is within the naturally occurring range (according to relevant literature: Persano Oddo, Apidologie 35 (2004), and Swiss food compendium (2004)). Dr. Martin Schubert Responsible Scientist, Certified Food Chemist

6 ANALYSIS REPORT No DATE: PAGE 1/ ANALYSIS REQUESTED: Electrical Conductivity ( ) Conductivity 0.35 ms/cm PM DE01_042 (a) 1 Regarding the examined parameter the sample corresponds to the legal regulations for Blossom honey. (Honey directive 2001/110/EC from Dec. 20th, 2001; Article 1 in connection with Annex II) Dr. Christof Kunert Responsible Scientist

7 ANALYSIS REPORT No DATE: PAGE 1/ Packaging / Quantity : Plastic container, twist off / ca.130g Start / End of analysis : / ANALYSIS REQUESTED: Chloramphenicol by ELISA-Screening-Test ( ) Chloramphenicol n.d. µg/kg PM DE01_024 (a) 1 n.d. - not detected < limit of quantification 0.3 µg/kg MRPL (Minimum Required Performance limit) for chloramphenicol = 0.3 µg/kg according to 2003/181/EG dated March 13, 2003 Regarding the examined parameter and with respect to the mentioned limit of quantification and the MRPL of 0.3 µg/kg the sample corresponds to the legal regulations (Regulation (EC) 470/2009 in conjunction with Regulation (EU) 37/2010 (dated Feb. 9th 2010)) and corresponds to the Decision 2003/181/EC dated March 13th, 2003 in connection with the Decision 2005/34/EC dated Jan. 11th, According to Decision 2002/657/EC the ELISA test shall only be used for screening purposes in conformity with Directive 96/23/EC. The rate of false negative results must be less than 5%. In case of a suspected positive result this result must be confirmed by a secondary confirmation method (LC-MS/MS). Dr. Martin Schubert Responsible Scientist, Certified Food Chemist

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